Exploring chemical analysis / Daniel C. Harris.
By: Harris, Daniel C.
Material type: BookPublisher: New York : W.H. Freeman and Co., 1997Description: xix, 476 p. : ill. (some col.) ; 26 cm.ISBN: 0716730421 .Subject(s): Chemistry, AnalyticDDC classification: 543Item type | Current library | Call number | Copy number | Status | Date due | Barcode | Item holds |
---|---|---|---|---|---|---|---|
General Lending | MTU Bishopstown Library Lending | 543 (Browse shelf(Opens below)) | 1 | Available | 00017765 | ||
General Lending | MTU Bishopstown Library Lending | 543 (Browse shelf(Opens below)) | 1 | Available | 00070830 | ||
General Lending | MTU Bishopstown Library Lending | 543 (Browse shelf(Opens below)) | 1 | Available | 00070829 |
Enhanced descriptions from Syndetics:
This text prepares students to use equipment they will encounter in professional labs in a variety of fields. Major topics covered include: statistics, volumetric analysis, spectrophotometry, acid-based equilibrium, electrochemistry and potentiometry, chromatography and electrophoresis, gravimetric and combustion analysis, and atomic spectroscopy. Lab experiments are included to give students hands-on practice using what they have learnt in the text.
Includes index.
Getting down to basics -- Tools of the trade -- Math toolkit -- Statistics -- A skirmish with equilibrium -- Good titrations -- Let there be light -- Spectrophotometry -- Monoprotic acid-base equilibria -- Buffers -- Acid-base titrations -- Polyprotic acids and bases -- Electrode potentials -- Electrode measurements -- EDTA and iodine titrations -- Principles of chromatography -- Gas and liquid chromatography -- Chromatography and capillary electrophoresis -- Gravimetric and combusion analysis -- Atomic-spectroscopy -- Experiments.
Table of contents provided by Syndetics
- Chapter 0 The Analytical Process Cocaine Use?
- Ask the River
- 0-1 The Analytical Chemist's Job
- 0-2 General Steps in a Chemical Analysis
- Box 0-1 Constructing a Representative Sample
- Chapter 1 Chemical Measurements Biochemical Measurements with a Nanoelectrode
- 1-1 SI Units and Prefixes
- Box 1-1 Exocytosis of Neurotransmitters
- 1-2 Conversion Between Units
- 1-3 Chemical Concentrations
- 1-4 Preparing Solutions
- 1-5 The Equilibrium Constant
- Chapter 2 Tools of the Trade A Quartz-Crystal Sensor with an Imprinted Layer for Yeast Cells
- 2-1 Safety, Waste Disposal, and Green Chemistry
- 2-2 Your Lab Notebook
- Box 2-1 Dan's Lab Notebook Entry
- 2-3 The Analytical Balance
- 2-4 Burets
- 2-5 Volumetric Flasks
- 2-6 Pipets and Syringes
- 2-7 Filtration
- 2-8 Drying
- 2-9 Calibration of Volumetric Glassware
- 2-10 Methods of Sample Preparation Reference Procedure: Calibrating a 50-mL buret
- Chapter 3 Math Toolkit Experimental Error
- 3-1 Significant Figures
- 3-2 Significant Figures in Arithmetic
- 3-3 Types of Error
- Box 3-1 What Are Standard Reference Materials?
- Box 3-2 Case Study: Systematic Error in Ozone Measurement
- 3-4 Propagation of Uncertainty
- 3-5 Introducing Spreadsheets
- 3-6 Graphing in Excel
- Chapter 4 Statistics Is My Red Blood Cell Count High Today?
- 4-1 The Gaussian Distribution
- 4-2 Student's t
- Box 4-1 Analytical Chemistry and the Law
- 4-3 Grubbs Test for an Outlier
- 4-4 Finding the "Best" Straight Line
- 4-5 Constructing a Calibration Curve
- 4-6 A Spreadsheet for Least Squares
- Chapter 5 Quality Assurance and Calibration Methods The Need for Quality Assurance
- 5-1 Basics of Quality Assurance
- Box 5-1 Control Charts
- 5-2 Validation of an Analytical Procedure
- 5-3 Standard Addition
- 5-4 Internal Standards
- Chapter 6 Good Titrations The Earliest Known Buret
- 6-1 Principles of Volumetric Analysis
- 6-2 Titration Calculations
- 6-3 Chemistry in a Fishtank
- Box 6-1 Studying a Marine Ecosystem
- 6-4 Solubility Product
- Box 6-2 The Logic of Approximations
- 6-5 Titration of a Mixture
- 6-6 Titrations Involving Silver Ion Demonstration
- 6-1 Fajans Titration
- Chapter 7 Gravimetric and Combustion Analysis
- The Geologic Time Scale and Gravimetric Analysis
- 7-1 Examples of Gravimetric Analysis
- Box 7-1 Shorthand for Organic Structures
- 7-2 Precipitation Demonstration
- 7-1 Colloids and Dialysis
- 7-3 Examples of Gravimetric Calculations
- 7-4 Combustion Analysis
- Chapter 8 Introducing Acids and Bases Acid Rain
- 8-1 What Are Acids and Bases?
- 8-2 Relation Between [H+], [OH-], and pH
- 8-3 Strengths of Acids and Bases Demonstration
- 8-1 HCl Fountain
- 8-4 pH